Sequence Summary Report Sequence name: 1120 compact LC.46 2018-04-20 17-01-36 (GMT +12-00).rst Description: Template sequence for two students Acquisition date: 4/21/2018 6:18:28 AM Approved by: Signature: Date: SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 1 of 54 Sequence Summary Report Sequence Table: Seq. Line: 1 Location: 1 Sample name: 0.000 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std000-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 2 Location: 1 Sample name: 0.000 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std000-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 3 Location: 2 Sample name: 0.016 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std016-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 4 Location: 2 Sample name: 0.016 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std016-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 2 of 54 Sequence Summary Report Seq. Line: 5 Location: 3 Sample name: 0.04 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std040-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 6 Location: 3 Sample name: 0.04 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std040-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 7 Location: 4 Sample name: 0.08 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std080-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 8 Location: 4 Sample name: 0.08 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std080-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 3 of 54 Sequence Summary Report Seq. Line: 9 Location: 5 Sample name: 0.16 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std160-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 10 Location: 5 Sample name: 0.16 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std160-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 11 Location: 6 Sample name: 0.4 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std400-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 12 Location: 6 Sample name: 0.4 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std400-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 4 of 54 Sequence Summary Report Seq. Line: 13 Location: 7 Sample name: 0.8 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std800-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 14 Location: 7 Sample name: 0.8 g/L Sample info: Method: CHEM225_hops_v02a. Data file Std800-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 15 Location: 100 Sample name: Wash Sample info: Method: CHEM225_hops_v02a. Data file Wash2-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 0.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 16 Location: 100 Sample name: Wash Sample info: Method: CHEM225_hops_v02a. Data file Wash2-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 0.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 5 of 54 Sequence Summary Report Seq. Line: 17 Location: 11 Sample name: High Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file High1-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 18 Location: 11 Sample name: High Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file High1-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 19 Location: 11 Sample name: High Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file High1-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 20 Location: 12 Sample name: Low Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file Low1-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 6 of 54 Sequence Summary Report Seq. Line: 21 Location: 12 Sample name: Low Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file Low1-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 22 Location: 12 Sample name: Low Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file Low1-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 23 Location: 13 Sample name: EE Low Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file EELow1-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 24 Location: 13 Sample name: EE Low Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file EELow1-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 7 of 54 Sequence Summary Report Seq. Line: 25 Location: 13 Sample name: EE Low Lawrence1 Sample info: Method: CHEM225_hops_v02a. Data file EELow1-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 26 Location: 21 Sample name: High Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file High2-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 27 Location: 21 Sample name: High Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file High2-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 28 Location: 21 Sample name: High Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file High2-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 8 of 54 Sequence Summary Report Seq. Line: 29 Location: 22 Sample name: Low Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file Low2-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 30 Location: 22 Sample name: Low Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file Low2-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 31 Location: 22 Sample name: Low Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file Low2-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 32 Location: 23 Sample name: EE Low Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file EELow2-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 9 of 54 Sequence Summary Report Seq. Line: 33 Location: 23 Sample name: EE Low Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file EELow2-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 34 Location: 23 Sample name: EE Low Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file EELow2-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 35 Location: 24 Sample name: EE High Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file EEHigh2-Rep1.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Seq. Line: 36 Location: 24 Sample name: EE High Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file EEHigh2-Rep2.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 10 of 54 Sequence Summary Report Seq. Line: 37 Location: 24 Sample name: EE High Ireland2 Sample info: Method: CHEM225_hops_v02a. Data file EEHigh2-Rep3.dat met Injection / Vial: 1 Inj. volume: 10.000 Sample type: Sample Calibration level: Update RT Undefined Update RF Undefined Bracketing: None Sample amount: 1.000 Lims ID: Multiplier: 1 Dilution: 1 Data file: Std000-Rep1.dat Sample name: 0.000 g/L Injection date: 4/20/2018 5:44:11 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 1 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 11 of 54 Sequence Summary Report Data file: Std000-Rep2.dat Sample name: 0.000 g/L Injection date: 4/20/2018 6:04:41 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 1 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 12 of 54 Sequence Summary Report Data file: Std016-Rep1.dat Sample name: 0.016 g/L Injection date: 4/20/2018 6:25:09 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 2 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.683 VWD: Signal A, 326 nm BV 16232 2561 0.00000 9.003 VWD: Signal A, 326 nm VB 3921586 424662 0.00000cohumulone 9.890 VWD: Signal A, 326 nm BV 8338931 755261 0.00000humulone-adhumulone 10.407 VWD: Signal A, 326 nm VV 135439 11650 0.00000 10.923 VWD: Signal A, 326 nm VV 60523 4061 0.00000 11.423 VWD: Signal A, 326 nm VV 3970035 334501 0.00000 11.967 VWD: Signal A, 326 nm VB 41072 3187 0.00000colupulone 12.800 VWD: Signal A, 326 nm BB 3046491 228337 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 13 of 54 Sequence Summary Report Data file: Std016-Rep2.dat Sample name: 0.016 g/L Injection date: 4/20/2018 6:45:35 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 2 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.687 VWD: Signal A, 326 nm BV 22004 3184 0.00000 9.003 VWD: Signal A, 326 nm VV 3999623 428573 0.00000cohumulone 9.893 VWD: Signal A, 326 nm VV 8417022 751355 0.00000humulone-adhumulone 10.410 VWD: Signal A, 326 nm VV 154468 12545 0.00000 10.923 VWD: Signal A, 326 nm VV 83220 5055 0.00000 11.423 VWD: Signal A, 326 nm VV 3988952 335157 0.00000 11.963 VWD: Signal A, 326 nm VB 41437 3300 0.00000colupulone 12.800 VWD: Signal A, 326 nm BB 3165908 229683 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 14 of 54 Sequence Summary Report Data file: Std040-Rep1.dat Sample name: 0.04 g/L Injection date: 4/20/2018 7:06:05 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 3 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 42748 6376 0.00000 9.000 VWD: Signal A, 326 nm VV 9188339 1000093 0.00000cohumulone 9.887 VWD: Signal A, 326 nm VV 19350344 1773736 0.00000humulone-adhumulone 10.410 VWD: Signal A, 326 nm VV 303226 26064 0.00000 10.917 VWD: Signal A, 326 nm VV 163031 10395 0.00000 11.423 VWD: Signal A, 326 nm VV 8844231 742518 0.00000 11.963 VWD: Signal A, 326 nm VB 93512 7692 0.00000colupulone 12.797 VWD: Signal A, 326 nm BB 7038262 509432 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 15 of 54 Sequence Summary Report Data file: Std040-Rep2.dat Sample name: 0.04 g/L Injection date: 4/20/2018 7:26:35 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 3 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.690 VWD: Signal A, 326 nm BV 43381 6483 0.00000 9.003 VWD: Signal A, 326 nm VV 9196225 1006633 0.00000cohumulone 9.890 VWD: Signal A, 326 nm VV 19359148 1754392 0.00000humulone-adhumulone 10.413 VWD: Signal A, 326 nm VV 299478 25642 0.00000 10.920 VWD: Signal A, 326 nm VV 159663 10230 0.00000 11.420 VWD: Signal A, 326 nm VV 8837544 746097 0.00000 11.963 VWD: Signal A, 326 nm VB 85982 7185 0.00000colupulone 12.797 VWD: Signal A, 326 nm BB 7076253 507416 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 16 of 54 Sequence Summary Report Data file: Std080-Rep1.dat Sample name: 0.08 g/L Injection date: 4/20/2018 7:47:03 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 4 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.687 VWD: Signal A, 326 nm BV 95234 13725 0.00000 9.000 VWD: Signal A, 326 nm VV 18276480 2002219 0.00000cohumulone 9.890 VWD: Signal A, 326 nm VV 38577069 3560448 0.00000humulone-adhumulone 10.413 VWD: Signal A, 326 nm VV 569924 49942 0.00000 10.920 VWD: Signal A, 326 nm VV 313707 20758 0.00000 11.423 VWD: Signal A, 326 nm VV 17957222 1509963 0.00000 11.970 VWD: Signal A, 326 nm VB 170324 14237 0.00000colupulone 12.800 VWD: Signal A, 326 nm BB 14486189 1031591 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 17 of 54 Sequence Summary Report Data file: Std080-Rep2.dat Sample name: 0.08 g/L Injection date: 4/20/2018 8:07:33 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 4 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.690 VWD: Signal A, 326 nm BV 87622 12980 0.00000 9.007 VWD: Signal A, 326 nm VV 18293402 2015237 0.00000cohumulone 9.893 VWD: Signal A, 326 nm VV 38594742 3533284 0.00000humulone-adhumulone 10.423 VWD: Signal A, 326 nm VV 563667 48875 0.00000 10.930 VWD: Signal A, 326 nm VV 307069 20430 0.00000 11.430 VWD: Signal A, 326 nm VV 17959054 1518020 0.00000colupulone 11.973 VWD: Signal A, 326 nm VB 165828 13705 0.00000 12.807 VWD: Signal A, 326 nm BE 14507120 1042371 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 18 of 54 Sequence Summary Report Data file: Std160-Rep1.dat Sample name: 0.16 g/L Injection date: 4/20/2018 8:27:59 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 5 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.687 VWD: Signal A, 326 nm BV 178390 26153 0.00000 9.003 VWD: Signal A, 326 nm VB 38437111 4244818 0.00000cohumulone 9.887 VWD: Signal A, 326 nm BV 81140554 7470707 0.00000humulone-adhumulone 10.420 VWD: Signal A, 326 nm VV 1120285 99198 0.00000 10.923 VWD: Signal A, 326 nm VV 628078 41259 0.00000 11.423 VWD: Signal A, 326 nm VV 36876250 3120153 0.00000 11.967 VWD: Signal A, 326 nm VB 353010 29140 0.00000colupulone 12.800 VWD: Signal A, 326 nm BE 29834902 2101546 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 19 of 54 Sequence Summary Report Data file: Std160-Rep2.dat Sample name: 0.16 g/L Injection date: 4/20/2018 8:48:24 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 5 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.683 VWD: Signal A, 326 nm BV 173173 26054 0.00000 8.997 VWD: Signal A, 326 nm VB 38471486 4260617 0.00000cohumulone 9.877 VWD: Signal A, 326 nm BV 81212729 7515717 0.00000humulone-adhumulone 10.410 VWD: Signal A, 326 nm VV 1094261 98229 0.00000 10.920 VWD: Signal A, 326 nm VV 601665 39820 0.00000 11.420 VWD: Signal A, 326 nm VV 36910263 3086732 0.00000 11.970 VWD: Signal A, 326 nm VB 336729 28183 0.00000colupulone 12.800 VWD: Signal A, 326 nm BE 29885381 2140503 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 20 of 54 Sequence Summary Report Data file: Std400-Rep1.dat Sample name: 0.4 g/L Injection date: 4/20/2018 9:08:52 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 6 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 381891 58236 0.00000 8.990 VWD: Signal A, 326 nm VB 88400434 9783693 0.00000cohumulone 9.867 VWD: Signal A, 326 nm BV 186633499 16982727 0.00000humulone-adhumulone 10.413 VWD: Signal A, 326 nm VV 2496292 221105 0.00000 10.923 VWD: Signal A, 326 nm VV 1460635 95375 0.00000 11.420 VWD: Signal A, 326 nm VV 84726109 7075797 0.00000 11.977 VWD: Signal A, 326 nm VB 784096 65006 0.00000colupulone 12.797 VWD: Signal A, 326 nm BE 68661835 4880136 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 21 of 54 Sequence Summary Report Data file: Std400-Rep2.dat Sample name: 0.4 g/L Injection date: 4/20/2018 9:29:16 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 6 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 364883 55668 0.00000 8.990 VWD: Signal A, 326 nm VB 88315757 9832967 0.00000cohumulone 9.867 VWD: Signal A, 326 nm BV 186609009 17023017 0.00000humulone-adhumulone 10.413 VWD: Signal A, 326 nm VV 2457943 220010 0.00000 10.920 VWD: Signal A, 326 nm VV 1431021 94916 0.00000 11.413 VWD: Signal A, 326 nm VV 84655580 7110679 0.00000 11.967 VWD: Signal A, 326 nm VB 778588 65586 0.00000colupulone 12.783 VWD: Signal A, 326 nm BE 68658784 4877124 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 22 of 54 Sequence Summary Report Data file: Std800-Rep1.dat Sample name: 0.8 g/L Injection date: 4/20/2018 9:49:41 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 7 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 734176 113394 0.00000 8.980 VWD: Signal A, 326 nm VB 175860910 19289034 0.00000cohumulone 9.843 VWD: Signal A, 326 nm BV 370045219 32945769 0.00000humulone-adhumulone 10.407 VWD: Signal A, 326 nm VV 4976578 440145 0.00000 10.907 VWD: Signal A, 326 nm VV 3007166 196448 0.00000 11.393 VWD: Signal A, 326 nm VV 168657806 14160727 0.00000 11.947 VWD: Signal A, 326 nm VB 1571590 132697 0.00000colupulone 12.750 VWD: Signal A, 326 nm BE 136852264 9618160 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 23 of 54 Sequence Summary Report Data file: Std800-Rep2.dat Sample name: 0.8 g/L Injection date: 4/20/2018 10:10:08 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 7 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 731593 115298 0.00000 8.980 VWD: Signal A, 326 nm VV 175655195 19302886 0.00000cohumulone 9.400 VWD: Signal A, 326 nm VB 288070 41684 0.00000 9.843 VWD: Signal A, 326 nm BV 370558259 33033229 0.00000humulone-adhumulone 10.407 VWD: Signal A, 326 nm VV 4902641 437125 0.00000 10.910 VWD: Signal A, 326 nm VV 2952293 193232 0.00000 11.390 VWD: Signal A, 326 nm VV 168599593 14147835 0.00000 11.950 VWD: Signal A, 326 nm VB 1519109 129722 0.00000colupulone 12.757 VWD: Signal A, 326 nm BE 137040977 9720901 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 24 of 54 Sequence Summary Report Data file: Wash2-Rep1.dat Sample name: Wash Injection date: 4/20/2018 10:30:05 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 100 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.027 VWD: Signal A, 326 nm BB 22787 2813 0.00000cohumulone 9.877 VWD: Signal A, 326 nm BB 227921 9854 0.00000humulone-adhumulone 12.613 VWD: Signal A, 326 nm BB 253263 10283 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 25 of 54 Sequence Summary Report Data file: Wash2-Rep2.dat Sample name: Wash Injection date: 4/20/2018 10:50:03 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 100 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.017 VWD: Signal A, 326 nm BB 13810 1851 0.00000cohumulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 26 of 54 Sequence Summary Report Data file: High1-Rep1.dat Sample name: High Lawrence1 Injection date: 4/20/2018 11:10:31 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 11 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.607 VWD: Signal A, 326 nm BV 106451 11159 0.00000 8.997 VWD: Signal A, 326 nm VB 25506908 2818634 0.00000cohumulone 9.877 VWD: Signal A, 326 nm BV 61460198 5950064 0.00000humulone-adhumulone 10.407 VWD: Signal A, 326 nm VV 430248 34878 0.00000 10.870 VWD: Signal A, 326 nm VV 1214017 80749 0.00000 11.410 VWD: Signal A, 326 nm VV 17320028 1472406 0.00000 11.953 VWD: Signal A, 326 nm VB 87453 6930 0.00000colupulone 12.780 VWD: Signal A, 326 nm BV 12078662 876977 0.00000lupulone-adlupulone 13.703 VWD: Signal A, 326 nm VE 17944 1857 0.00000 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 27 of 54 Sequence Summary Report Data file: High1-Rep2.dat Sample name: High Lawrence1 Injection date: 4/20/2018 11:31:04 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 11 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.603 VWD: Signal A, 326 nm BV 95333 10475 0.00000 9.000 VWD: Signal A, 326 nm VV 25462405 2817831 0.00000cohumulone 9.880 VWD: Signal A, 326 nm VV 61480658 5977169 0.00000humulone-adhumulone 10.413 VWD: Signal A, 326 nm VV 386320 32836 0.00000 10.877 VWD: Signal A, 326 nm VV 1036816 74680 0.00000 11.420 VWD: Signal A, 326 nm VV 17245838 1471986 0.00000 11.953 VWD: Signal A, 326 nm VB 143746 10080 0.00000colupulone 12.787 VWD: Signal A, 326 nm BB 11939943 884026 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 28 of 54 Sequence Summary Report Data file: High1-Rep3.dat Sample name: High Lawrence1 Injection date: 4/20/2018 11:51:32 PM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 11 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.607 VWD: Signal A, 326 nm BV 97336 10617 0.00000 9.000 VWD: Signal A, 326 nm VV 25432929 2808573 0.00000cohumulone 9.883 VWD: Signal A, 326 nm VV 61391144 5957701 0.00000humulone-adhumulone 10.417 VWD: Signal A, 326 nm VV 377986 31888 0.00000 10.880 VWD: Signal A, 326 nm VV 1039678 75040 0.00000 11.427 VWD: Signal A, 326 nm VV 17148725 1456672 0.00000 11.970 VWD: Signal A, 326 nm VB 129637 9047 0.00000colupulone 12.797 VWD: Signal A, 326 nm BB 11910208 884854 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 29 of 54 Sequence Summary Report Data file: Low1-Rep1.dat Sample name: Low Lawrence1 Injection date: 4/21/2018 12:12:02 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 12 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.683 VWD: Signal A, 326 nm IV 219782 24492 0.00000 9.003 VWD: Signal A, 326 nm VV 9742978 927459 0.00000cohumulone 9.887 VWD: Signal A, 326 nm VV 25676466 2419365 0.00000humulone-adhumulone 10.417 VWD: Signal A, 326 nm VV 926726 86112 0.00000 10.867 VWD: Signal A, 326 nm VV 1949027 98080 0.00000 11.423 VWD: Signal A, 326 nm VV 21455851 1870298 0.00000 11.967 VWD: Signal A, 326 nm VV 721822 50133 0.00000colupulone 12.797 VWD: Signal A, 326 nm VE 32124626 2356733 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 30 of 54 Sequence Summary Report Data file: Low1-Rep2.dat Sample name: Low Lawrence1 Injection date: 4/21/2018 12:32:28 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 12 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.687 VWD: Signal A, 326 nm IV 224521 25067 0.00000 9.003 VWD: Signal A, 326 nm VV 9815987 924485 0.00000cohumulone 9.890 VWD: Signal A, 326 nm VV 25678575 2417004 0.00000humulone-adhumulone 10.423 VWD: Signal A, 326 nm VV 934882 85773 0.00000 10.873 VWD: Signal A, 326 nm VV 1983606 99503 0.00000 11.427 VWD: Signal A, 326 nm VV 21515453 1868330 0.00000colupulone 11.973 VWD: Signal A, 326 nm VV 705710 49151 0.00000 12.800 VWD: Signal A, 326 nm VV 31981483 2342243 0.00000lupulone-adlupulone 13.513 VWD: Signal A, 326 nm VE 172465 9528 0.00000 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 31 of 54 Sequence Summary Report Data file: Low1-Rep3.dat Sample name: Low Lawrence1 Injection date: 4/21/2018 12:52:53 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 12 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.683 VWD: Signal A, 326 nm IV 221202 24545 0.00000 9.007 VWD: Signal A, 326 nm VV 9832056 924282 0.00000cohumulone 9.890 VWD: Signal A, 326 nm VV 25724422 2401885 0.00000humulone-adhumulone 10.420 VWD: Signal A, 326 nm VV 936110 86331 0.00000 10.870 VWD: Signal A, 326 nm VV 1952308 97262 0.00000 11.423 VWD: Signal A, 326 nm VV 21501141 1879498 0.00000 11.970 VWD: Signal A, 326 nm VB 678200 49106 0.00000colupulone 12.803 VWD: Signal A, 326 nm BB 31597673 2360424 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 32 of 54 Sequence Summary Report Data file: EELow1-Rep1.dat Sample name: EE Low Lawrence1 Injection date: 4/21/2018 1:13:19 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 13 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.020 VWD: Signal A, 326 nm BB 94468 9647 0.00000cohumulone 9.900 VWD: Signal A, 326 nm BB 314127 25044 0.00000humulone-adhumulone 11.440 VWD: Signal A, 326 nm BB 109064 9931 0.00000colupulone 12.793 VWD: Signal A, 326 nm BB 301893 16335 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 33 of 54 Sequence Summary Report Data file: EELow1-Rep2.dat Sample name: EE Low Lawrence1 Injection date: 4/21/2018 1:33:42 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 13 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.007 VWD: Signal A, 326 nm BV 89212 8760 0.00000cohumulone 9.893 VWD: Signal A, 326 nm VB 327970 23411 0.00000humulone-adhumulone 11.427 VWD: Signal A, 326 nm BB 104080 9550 0.00000colupulone 12.807 VWD: Signal A, 326 nm BB 160212 12290 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 34 of 54 Sequence Summary Report Data file: EELow1-Rep3.dat Sample name: EE Low Lawrence1 Injection date: 4/21/2018 1:54:10 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 13 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.007 VWD: Signal A, 326 nm BB 78033 8586 0.00000cohumulone 9.897 VWD: Signal A, 326 nm BB 219231 21323 0.00000humulone-adhumulone 11.427 VWD: Signal A, 326 nm BB 110793 10007 0.00000colupulone 12.807 VWD: Signal A, 326 nm BB 155863 11800 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 35 of 54 Sequence Summary Report Data file: High2-Rep1.dat Sample name: High Ireland2 Injection date: 4/21/2018 2:14:39 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 21 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.590 VWD: Signal A, 326 nm IV 240709 26048 0.00000 8.977 VWD: Signal A, 326 nm VB 58221982 6392442 0.00000cohumulone 9.857 VWD: Signal A, 326 nm BV 140357090 13494175 0.00000humulone-adhumulone 10.400 VWD: Signal A, 326 nm VV 898915 74067 0.00000 10.867 VWD: Signal A, 326 nm VV 2448169 179092 0.00000 11.410 VWD: Signal A, 326 nm VV 38882223 3290134 0.00000 11.957 VWD: Signal A, 326 nm VB 203922 15619 0.00000colupulone 12.790 VWD: Signal A, 326 nm BE 29146553 2105321 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 36 of 54 Sequence Summary Report Data file: High2-Rep2.dat Sample name: High Ireland2 Injection date: 4/21/2018 2:35:08 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 21 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.610 VWD: Signal A, 326 nm BV 281286 29074 0.00000 8.997 VWD: Signal A, 326 nm VB 58153512 6444032 0.00000cohumulone 9.873 VWD: Signal A, 326 nm BV 140168040 13430195 0.00000humulone-adhumulone 10.420 VWD: Signal A, 326 nm VV 816901 69062 0.00000 10.887 VWD: Signal A, 326 nm VV 2358005 177524 0.00000 11.430 VWD: Signal A, 326 nm VV 38685787 3244246 0.00000colupulone 11.980 VWD: Signal A, 326 nm VV 258835 18474 0.00000 12.800 VWD: Signal A, 326 nm VV 28999216 2119019 0.00000lupulone-adlupulone 13.717 VWD: Signal A, 326 nm VE 51803 5050 0.00000 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 37 of 54 Sequence Summary Report Data file: High2-Rep3.dat Sample name: High Ireland2 Injection date: 4/21/2018 2:55:40 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 21 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.613 VWD: Signal A, 326 nm BV 280220 29404 0.00000 8.997 VWD: Signal A, 326 nm VB 58170643 6480320 0.00000cohumulone 9.873 VWD: Signal A, 326 nm BV 140255120 13510774 0.00000humulone-adhumulone 10.420 VWD: Signal A, 326 nm VV 778620 67572 0.00000 10.883 VWD: Signal A, 326 nm VV 2285234 174404 0.00000 11.427 VWD: Signal A, 326 nm VV 38581016 3294234 0.00000colupulone 11.980 VWD: Signal A, 326 nm VB 215610 15905 0.00000 12.803 VWD: Signal A, 326 nm BB 28570123 2089232 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 38 of 54 Sequence Summary Report Data file: Low2-Rep1.dat Sample name: Low Ireland2 Injection date: 4/21/2018 3:16:06 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 22 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 202566 23669 0.00000 9.003 VWD: Signal A, 326 nm VV 22441118 2413969 0.00000cohumulone 9.883 VWD: Signal A, 326 nm VV 60076192 5866263 0.00000humulone-adhumulone 10.420 VWD: Signal A, 326 nm VV 486761 45744 0.00000 10.893 VWD: Signal A, 326 nm VV 976854 64034 0.00000 11.430 VWD: Signal A, 326 nm VV 25130728 2173933 0.00000colupulone 11.990 VWD: Signal A, 326 nm VV 308462 19198 0.00000 12.803 VWD: Signal A, 326 nm VV 25309949 1860143 0.00000lupulone-adlupulone 13.500 VWD: Signal A, 326 nm VE 175927 8669 0.00000 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 39 of 54 Sequence Summary Report Data file: Low2-Rep2.dat Sample name: Low Ireland2 Injection date: 4/21/2018 3:36:32 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 22 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.680 VWD: Signal A, 326 nm BV 204884 24229 0.00000 9.000 VWD: Signal A, 326 nm VV 22360105 2397088 0.00000cohumulone 9.883 VWD: Signal A, 326 nm VV 59801115 5844744 0.00000humulone-adhumulone 10.420 VWD: Signal A, 326 nm VV 505595 46767 0.00000 10.890 VWD: Signal A, 326 nm VV 974261 64034 0.00000 11.430 VWD: Signal A, 326 nm VV 25032441 2162588 0.00000colupulone 11.983 VWD: Signal A, 326 nm VV 190879 14418 0.00000 12.803 VWD: Signal A, 326 nm VV 25182560 1861600 0.00000lupulone-adlupulone 13.487 VWD: Signal A, 326 nm VE 187990 9976 0.00000 SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 40 of 54 Sequence Summary Report Data file: Low2-Rep3.dat Sample name: Low Ireland2 Injection date: 4/21/2018 3:56:58 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 22 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [] 8.683 VWD: Signal A, 326 nm BV 203286 24210 0.00000 9.000 VWD: Signal A, 326 nm VB 22385449 2401534 0.00000cohumulone 9.887 VWD: Signal A, 326 nm BV 59893721 5813245 0.00000humulone-adhumulone 10.423 VWD: Signal A, 326 nm VV 540853 48667 0.00000 10.893 VWD: Signal A, 326 nm VV 1009618 65262 0.00000 11.433 VWD: Signal A, 326 nm VV 25102264 2147747 0.00000colupulone 11.980 VWD: Signal A, 326 nm VB 192066 14910 0.00000 12.807 VWD: Signal A, 326 nm BB 24868075 1857592 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 41 of 54 Sequence Summary Report Data file: EELow2-Rep1.dat Sample name: EE Low Ireland2 Injection date: 4/21/2018 4:17:24 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 23 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.007 VWD: Signal A, 326 nm BV 143513 14980 0.00000cohumulone 9.893 VWD: Signal A, 326 nm VB 548149 38039 0.00000humulone-adhumulone 11.440 VWD: Signal A, 326 nm BB 53285 5088 0.00000colupulone 12.787 VWD: Signal A, 326 nm BB 184403 8879 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 42 of 54 Sequence Summary Report Data file: EELow2-Rep2.dat Sample name: EE Low Ireland2 Injection date: 4/21/2018 4:37:49 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 23 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 8.987 VWD: Signal A, 326 nm BB 116243 13459 0.00000cohumulone 9.873 VWD: Signal A, 326 nm BB 354703 32567 0.00000humulone-adhumulone 11.410 VWD: Signal A, 326 nm BB 57108 5403 0.00000colupulone 12.777 VWD: Signal A, 326 nm BB 65376 5133 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 43 of 54 Sequence Summary Report Data file: EELow2-Rep3.dat Sample name: EE Low Ireland2 Injection date: 4/21/2018 4:58:14 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 23 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.010 VWD: Signal A, 326 nm BB 126742 14200 0.00000cohumulone 9.897 VWD: Signal A, 326 nm BB 329971 31930 0.00000humulone-adhumulone 11.430 VWD: Signal A, 326 nm BB 59428 5266 0.00000colupulone 12.810 VWD: Signal A, 326 nm BB 72804 5700 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 44 of 54 Sequence Summary Report Data file: EEHigh2-Rep1.dat Sample name: EE High Ireland2 Injection date: 4/21/2018 5:18:41 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 24 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 1 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.007 VWD: Signal A, 326 nm BB 339496 38514 0.00000cohumulone 9.897 VWD: Signal A, 326 nm BB 868063 83322 0.00000humulone-adhumulone 11.437 VWD: Signal A, 326 nm BB 196628 16695 0.00000colupulone 12.807 VWD: Signal A, 326 nm BB 131961 10491 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 45 of 54 Sequence Summary Report Data file: EEHigh2-Rep2.dat Sample name: EE High Ireland2 Injection date: 4/21/2018 5:39:12 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 24 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 2 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.010 VWD: Signal A, 326 nm BB 344308 39037 0.00000cohumulone 9.897 VWD: Signal A, 326 nm BB 863307 82683 0.00000humulone-adhumulone 11.440 VWD: Signal A, 326 nm BB 194503 16825 0.00000colupulone 12.813 VWD: Signal A, 326 nm BB 136859 10638 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 46 of 54 Sequence Summary Report Data file: EEHigh2-Rep3.dat Sample name: EE High Ireland2 Injection date: 4/21/2018 5:59:39 AM Sample type: Sample Acq. method: C:\Enterprise\Projects\C Location: 24 HEM225\Hops Lab\Methods\CHEM225 _hops_v02a.met Analysis method: CHEM225_hops_v0 Injection: 3 2a.met Acq. operator: SYSTEM (SYSTEM) Injection volume: 10.000 Last changed: 4/10/2017 2:19:40 PM RT [min] Signal Type Area Height AmountName [ppm] 9.003 VWD: Signal A, 326 nm BB 338606 38961 0.00000cohumulone 9.890 VWD: Signal A, 326 nm BB 863238 83434 0.00000humulone-adhumulone 11.420 VWD: Signal A, 326 nm BB 192337 16630 0.00000colupulone 12.800 VWD: Signal A, 326 nm BB 151945 11481 0.00000lupulone-adlupulone SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 47 of 54 Sequence Summary Report Sample Summary Line# Inj# Location Sample Name Sample Amt Multiplier * Datafile Cal Lvl Dilution 1 1 10.000 g/L 1.0000 1.0000 Std000-Rep1.dat 2 1 10.000 g/L 1.0000 1.0000 Std000-Rep2.dat 3 1 20.016 g/L 1.0000 1.0000 Std016-Rep1.dat 4 1 20.016 g/L 1.0000 1.0000 Std016-Rep2.dat 5 1 30.04 g/L 1.0000 1.0000 Std040-Rep1.dat 6 1 30.04 g/L 1.0000 1.0000 Std040-Rep2.dat 7 1 40.08 g/L 1.0000 1.0000 Std080-Rep1.dat 8 1 40.08 g/L 1.0000 1.0000 Std080-Rep2.dat 9 1 50.16 g/L 1.0000 1.0000 Std160-Rep1.dat 10 1 50.16 g/L 1.0000 1.0000 Std160-Rep2.dat 11 1 60.4 g/L 1.0000 1.0000 Std400-Rep1.dat 12 1 60.4 g/L 1.0000 1.0000 Std400-Rep2.dat 13 1 70.8 g/L 1.0000 1.0000 Std800-Rep1.dat 14 1 70.8 g/L 1.0000 1.0000 Std800-Rep2.dat 15 1 100Wash 1.0000 Wash2-Rep1.dat 16 2 100Wash 1.0000 Wash2-Rep2.dat 17 1 11High Lawrence1 1.0000 1.0000 High1-Rep1.dat 18 2 11High Lawrence1 1.0000 1.0000 High1-Rep2.dat 19 3 11High Lawrence1 1.0000 1.0000 High1-Rep3.dat 20 1 12Low Lawrence1 1.0000 1.0000 Low1-Rep1.dat 21 2 12Low Lawrence1 1.0000 1.0000 Low1-Rep2.dat 22 3 12Low Lawrence1 1.0000 1.0000 Low1-Rep3.dat 23 1 13EE Low Lawrence1 1.0000 1.0000 EELow1-Rep1.dat 24 2 13EE Low Lawrence1 1.0000 1.0000 EELow1-Rep2.dat 25 3 13EE Low Lawrence1 1.0000 1.0000 EELow1-Rep3.dat 26 1 21High Ireland2 1.0000 1.0000 High2-Rep1.dat 27 2 21High Ireland2 1.0000 1.0000 High2-Rep2.dat 28 3 21High Ireland2 1.0000 1.0000 High2-Rep3.dat 29 1 22Low Ireland2 1.0000 1.0000 Low2-Rep1.dat 30 2 22Low Ireland2 1.0000 1.0000 Low2-Rep2.dat 31 3 22Low Ireland2 1.0000 1.0000 Low2-Rep3.dat 32 1 23EE Low Ireland2 1.0000 1.0000 EELow2-Rep1.dat 33 2 23EE Low Ireland2 1.0000 1.0000 EELow2-Rep2.dat 34 3 23EE Low Ireland2 1.0000 1.0000 EELow2-Rep3.dat 35 1 24EE High Ireland2 1.0000 1.0000 EEHigh2-Rep1.dat 36 2 24EE High Ireland2 1.0000 1.0000 EEHigh2-Rep2.dat 37 3 24EE High Ireland2 1.0000 1.0000 EEHigh2-Rep3.dat SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 48 of 54 Sequence Summary Report Calibration sample statistics: Compound: Signal: VWD: Signal A, 326 nm Statistic results not available Compound: cohumulone Signal: VWD: Signal A, 326 nm Statistic results not available Compound: humulone-adhumulone Signal: VWD: Signal A, 326 nm Statistic results not available Compound: colupulone Signal: VWD: Signal A, 326 nm Statistic results not available Compound: lupulone-adlupulone Signal: VWD: Signal A, 326 nm Statistic results not available SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 49 of 54 Sequence Summary Report Sample statistics: Compound: Signal: VWD: Signal A, 326 nm Statistic results not available SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 50 of 54 Sequence Summary Report Compound: cohumulone Signal: VWD: Signal A, 326 nm Line# Inj# Type RT [min] Amount Area Height Tail F.Sample Name [ppm] 3 1 VB 9.003 0.00000 3921586 424662 0.000.016 g/L 4 1 VV 9.003 0.00000 3999623 428573 0.000.016 g/L 5 1 VV 9.000 0.00000 9188339 1000093 0.000.04 g/L 6 1 VV 9.003 0.00000 9196225 1006633 0.000.04 g/L 7 1 VV 9.000 0.00000 18276480 2002219 0.000.08 g/L 8 1 VV 9.007 0.00000 18293402 2015237 0.000.08 g/L 9 1 VB 9.003 0.00000 38437111 4244818 0.000.16 g/L 10 1 VB 8.997 0.00000 38471486 4260617 0.000.16 g/L 11 1 VB 8.990 0.00000 88400434 9783693 0.000.4 g/L 12 1 VB 8.990 0.00000 88315757 9832967 0.000.4 g/L 13 1 VB 8.980 0.00000 175860910 19289034 0.000.8 g/L 14 1 VV 8.980 0.00000 175655195 19302886 0.000.8 g/L 15 1 BB 9.027 0.00000 22787 2813 0.00Wash 16 2 BB 9.017 0.00000 13810 1851 0.00Wash 17 1 VB 8.997 0.00000 25506908 2818634 0.00High Lawrence1 18 2 VV 9.000 0.00000 25462405 2817831 0.00High Lawrence1 19 3 VV 9.000 0.00000 25432929 2808573 0.00High Lawrence1 20 1 VV 9.003 0.00000 9742978 927459 0.00Low Lawrence1 21 2 VV 9.003 0.00000 9815987 924485 0.00Low Lawrence1 22 3 VV 9.007 0.00000 9832056 924282 0.00Low Lawrence1 23 1 BB 9.020 0.00000 94468 9647 0.00EE Low Lawrence1 24 2 BV 9.007 0.00000 89212 8760 0.00EE Low Lawrence1 25 3 BB 9.007 0.00000 78033 8586 0.00EE Low Lawrence1 26 1 VB 8.977 0.00000 58221982 6392442 0.00High Ireland2 27 2 VB 8.997 0.00000 58153512 6444032 0.00High Ireland2 28 3 VB 8.997 0.00000 58170643 6480320 0.00High Ireland2 29 1 VV 9.003 0.00000 22441118 2413969 0.00Low Ireland2 30 2 VV 9.000 0.00000 22360105 2397088 0.00Low Ireland2 31 3 VB 9.000 0.00000 22385449 2401534 0.00Low Ireland2 32 1 BV 9.007 0.00000 143513 14980 0.00EE Low Ireland2 33 2 BB 8.987 0.00000 116243 13459 0.00EE Low Ireland2 34 3 BB 9.010 0.00000 126742 14200 0.00EE Low Ireland2 35 1 BB 9.007 0.00000 339496 38514 0.00EE High Ireland2 36 2 BB 9.010 0.00000 344308 39037 0.00EE High Ireland2 37 3 BB 9.003 0.00000 338606 38961 0.00EE High Ireland2 Average 9.001 0.00000 29064281 3186654 0.00 Standard 0.0104 0.00000 43908755.6 4839633.71 0.00 RSD 0.115 NaN 151.075 151.872 NaN SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 51 of 54 Sequence Summary Report Compound: humulone-adhumulone Signal: VWD: Signal A, 326 nm Line# Inj# Type RT [min] Amount Area Height Tail F.Sample Name [] 3 1 BV 9.890 0.00000 8338931 755261 0.000.016 g/L 4 1 VV 9.893 0.00000 8417022 751355 0.000.016 g/L 5 1 VV 9.887 0.00000 19350344 1773736 0.000.04 g/L 6 1 VV 9.890 0.00000 19359148 1754392 0.000.04 g/L 7 1 VV 9.890 0.00000 38577069 3560448 0.000.08 g/L 8 1 VV 9.893 0.00000 38594742 3533284 0.000.08 g/L 9 1 BV 9.887 0.00000 81140554 7470707 0.000.16 g/L 10 1 BV 9.877 0.00000 81212729 7515717 0.000.16 g/L 11 1 BV 9.867 0.00000 186633499 16982727 0.000.4 g/L 12 1 BV 9.867 0.00000 186609009 17023017 0.000.4 g/L 13 1 BV 9.843 0.00000 370045219 32945769 0.000.8 g/L 14 1 BV 9.843 0.00000 370558259 33033229 0.000.8 g/L 15 1 BB 9.877 0.00000 227921 9854 0.00Wash 17 1 BV 9.877 0.00000 61460198 5950064 0.00High Lawrence1 18 2 VV 9.880 0.00000 61480658 5977169 0.00High Lawrence1 19 3 VV 9.883 0.00000 61391144 5957701 0.00High Lawrence1 20 1 VV 9.887 0.00000 25676466 2419365 0.00Low Lawrence1 21 2 VV 9.890 0.00000 25678575 2417004 0.00Low Lawrence1 22 3 VV 9.890 0.00000 25724422 2401885 0.00Low Lawrence1 23 1 BB 9.900 0.00000 314127 25044 0.00EE Low Lawrence1 24 2 VB 9.893 0.00000 327970 23411 0.00EE Low Lawrence1 25 3 BB 9.897 0.00000 219231 21323 0.00EE Low Lawrence1 26 1 BV 9.857 0.00000 140357090 13494175 0.00High Ireland2 27 2 BV 9.873 0.00000 140168040 13430195 0.00High Ireland2 28 3 BV 9.873 0.00000 140255120 13510774 0.00High Ireland2 29 1 VV 9.883 0.00000 60076192 5866263 0.00Low Ireland2 30 2 VV 9.883 0.00000 59801115 5844744 0.00Low Ireland2 31 3 BV 9.887 0.00000 59893721 5813245 0.00Low Ireland2 32 1 VB 9.893 0.00000 548149 38039 0.00EE Low Ireland2 33 2 BB 9.873 0.00000 354703 32567 0.00EE Low Ireland2 34 3 BB 9.897 0.00000 329971 31930 0.00EE Low Ireland2 35 1 BB 9.897 0.00000 868063 83322 0.00EE High Ireland2 36 2 BB 9.897 0.00000 863307 82683 0.00EE High Ireland2 37 3 BB 9.890 0.00000 863238 83434 0.00EE High Ireland2 Average 9.882 0.00000 66932822 6194525 0.00 Standard 0.0141 0.00000 94022771.6 8468238.19 0.00 RSD 0.143 NaN 140.473 136.705 NaN SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 52 of 54 Sequence Summary Report Compound: colupulone Signal: VWD: Signal A, 326 nm Line# Inj# Type RT [min] Amount Area Height Tail F.Sample Name [] 3 1 VB 11.967 0.00000 41072 3187 0.000.016 g/L 4 1 VB 11.963 0.00000 41437 3300 0.000.016 g/L 5 1 VB 11.963 0.00000 93512 7692 0.000.04 g/L 6 1 VB 11.963 0.00000 85982 7185 0.000.04 g/L 7 1 VB 11.970 0.00000 170324 14237 0.000.08 g/L 8 1 VV 11.430 0.00000 17959054 1518020 0.000.08 g/L 9 1 VB 11.967 0.00000 353010 29140 0.000.16 g/L 10 1 VB 11.970 0.00000 336729 28183 0.000.16 g/L 11 1 VB 11.977 0.00000 784096 65006 0.000.4 g/L 12 1 VB 11.967 0.00000 778588 65586 0.000.4 g/L 13 1 VB 11.947 0.00000 1571590 132697 0.000.8 g/L 14 1 VB 11.950 0.00000 1519109 129722 0.000.8 g/L 17 1 VB 11.953 0.00000 87453 6930 0.00High Lawrence1 18 2 VB 11.953 0.00000 143746 10080 0.00High Lawrence1 19 3 VB 11.970 0.00000 129637 9047 0.00High Lawrence1 20 1 VV 11.967 0.00000 721822 50133 0.00Low Lawrence1 21 2 VV 11.427 0.00000 21515453 1868330 0.00Low Lawrence1 22 3 VB 11.970 0.00000 678200 49106 0.00Low Lawrence1 23 1 BB 11.440 0.00000 109064 9931 0.00EE Low Lawrence1 24 2 BB 11.427 0.00000 104080 9550 0.00EE Low Lawrence1 25 3 BB 11.427 0.00000 110793 10007 0.00EE Low Lawrence1 26 1 VB 11.957 0.00000 203922 15619 0.00High Ireland2 27 2 VV 11.430 0.00000 38685787 3244246 0.00High Ireland2 28 3 VV 11.427 0.00000 38581016 3294234 0.00High Ireland2 29 1 VV 11.430 0.00000 25130728 2173933 0.00Low Ireland2 30 2 VV 11.430 0.00000 25032441 2162588 0.00Low Ireland2 31 3 VV 11.433 0.00000 25102264 2147747 0.00Low Ireland2 32 1 BB 11.440 0.00000 53285 5088 0.00EE Low Ireland2 33 2 BB 11.410 0.00000 57108 5403 0.00EE Low Ireland2 34 3 BB 11.430 0.00000 59428 5266 0.00EE Low Ireland2 35 1 BB 11.437 0.00000 196628 16695 0.00EE High Ireland2 36 2 BB 11.440 0.00000 194503 16825 0.00EE High Ireland2 37 3 BB 11.420 0.00000 192337 16630 0.00EE High Ireland2 Average 11.705 0.00000 6085582 519132 0.00 Standard 0.271 0.00000 11784797.3 1005389.71 0.00 RSD 2.314 NaN 193.651 193.668 NaN SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 53 of 54 Sequence Summary Report Compound: lupulone-adlupulone Signal: VWD: Signal A, 326 nm Line# Inj# Type RT [min] Amount Area Height Tail F.Sample Name [] 3 1 BB 12.800 0.00000 3046491 228337 0.000.016 g/L 4 1 BB 12.800 0.00000 3165908 229683 0.000.016 g/L 5 1 BB 12.797 0.00000 7038262 509432 0.000.04 g/L 6 1 BB 12.797 0.00000 7076253 507416 0.000.04 g/L 7 1 BB 12.800 0.00000 14486189 1031591 0.000.08 g/L 8 1 BE 12.807 0.00000 14507120 1042371 0.000.08 g/L 9 1 BE 12.800 0.00000 29834902 2101546 0.000.16 g/L 10 1 BE 12.800 0.00000 29885381 2140503 0.000.16 g/L 11 1 BE 12.797 0.00000 68661835 4880136 0.000.4 g/L 12 1 BE 12.783 0.00000 68658784 4877124 0.000.4 g/L 13 1 BE 12.750 0.00000 136852264 9618160 0.000.8 g/L 14 1 BE 12.757 0.00000 137040977 9720901 0.000.8 g/L 15 1 BB 12.613 0.00000 253263 10283 0.00Wash 17 1 BV 12.780 0.00000 12078662 876977 0.00High Lawrence1 18 2 BB 12.787 0.00000 11939943 884026 0.00High Lawrence1 19 3 BB 12.797 0.00000 11910208 884854 0.00High Lawrence1 20 1 VE 12.797 0.00000 32124626 2356733 0.00Low Lawrence1 21 2 VV 12.800 0.00000 31981483 2342243 0.00Low Lawrence1 22 3 BB 12.803 0.00000 31597673 2360424 0.00Low Lawrence1 23 1 BB 12.793 0.00000 301893 16335 0.00EE Low Lawrence1 24 2 BB 12.807 0.00000 160212 12290 0.00EE Low Lawrence1 25 3 BB 12.807 0.00000 155863 11800 0.00EE Low Lawrence1 26 1 BE 12.790 0.00000 29146553 2105321 0.00High Ireland2 27 2 VV 12.800 0.00000 28999216 2119019 0.00High Ireland2 28 3 BB 12.803 0.00000 28570123 2089232 0.00High Ireland2 29 1 VV 12.803 0.00000 25309949 1860143 0.00Low Ireland2 30 2 VV 12.803 0.00000 25182560 1861600 0.00Low Ireland2 31 3 BB 12.807 0.00000 24868075 1857592 0.00Low Ireland2 32 1 BB 12.787 0.00000 184403 8879 0.00EE Low Ireland2 33 2 BB 12.777 0.00000 65376 5133 0.00EE Low Ireland2 34 3 BB 12.810 0.00000 72804 5700 0.00EE Low Ireland2 35 1 BB 12.807 0.00000 131961 10491 0.00EE High Ireland2 36 2 BB 12.813 0.00000 136859 10638 0.00EE High Ireland2 37 3 BB 12.800 0.00000 151945 11481 0.00EE High Ireland2 Average 12.790 0.00000 23987589 1723188 0.00 Standard 0.0341 0.00000 33745804.2 2387019.58 0.00 RSD 0.267 NaN 140.680 138.523 NaN SequenceSummary_Standard.rdl [0] Printed: 4/21/2018 6:18:34 AM Page 54 of 54