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Synthesis of BBG-2020-11 #11
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Here is the data from the 1H NMR experiment on BGG-2020-11 (see below for structure). I’ve also added this to this repository along with the raw NMR data. For 11A - I found that it was appeared to be soluble in methanol but when I did a 1H NMR experiment in MeOD I saw no signals. I can try to do look at the mass if you like but I'm may not see much. For 11B - The spectra indicated that there may be product but the integration is off. It would be worth trying to get a pure sample and doing further analysis on it to be sure that we have the product we are expecting. NMR Data |
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